JOURNAL OF SHANDONG UNIVERSITY (ENGINEERING SCIENCE) ›› 2010, Vol. 40 ›› Issue (1): 108-114.

• Articles • Previous Articles     Next Articles

Synthesis process of long-chain alkyl amide imidazoline by React IRTM

  

  1. School of Chemistry and Chemical Engineering, Shandong University, Jinan 250061, China
  • Received:2009-03-23 Online:2010-02-16 Published:2009-03-23
  • Contact: YU Ping(1963-), female, born in Shandong Weihai, associated professor, her rsearch interests mainly focuse in chemical engineering.
  • About author:ZHANG Lei(1984-), male, Born in Anhui Huaibei, master graduates, his research interests mainly focuse in functional polymer material.E-mail:98844889@163.com
  • Supported by:

    This work was supported by the National Key Foundation Theory Study of China(2008CB617508)

Abstract:

With a special structure containing two nitrogen atoms in its fivemembered heterocyclic ring, imidazoline may become a new chemical with special feature by introducing other functional groups during its synthesis process. It is the hotspot research in the field of synthesis of functional macromolecule materials at present. In this paper, imidazoline was synthesized by stearic acid and diethylenetriamine, and a series of functional groups spectrum during the reaction process were obtained by using the react IR analytical system (React IRTM). By analyzing the changes of spectrum of the characteristic functional groups, the mechanism and process of synthesis reaction were discussed. The results showed that the mixing process of raw materials at the initial process was a physicochemical reaction process, and there was a lowest value area of the target product in the reaction process. As a result, the reaction of introducing other functional groups to this functional group should not take place in this lowest value area.

Key words: React IRTM; imidazoline; acylami

No related articles found!
Viewed
Full text
157
HTML PDF
Just accepted Online first Issue Just accepted Online first Issue
0 0 0 0 0 157

  From Others local
  Times 3 154
  Rate 2% 98%

Abstract
922
Just accepted Online first Issue
0 0 922
  From Others local
  Times 917 5
  Rate 99% 1%

Cited

Web of Science  Crossref   ScienceDirect  Search for Citations in Google Scholar >>
 
This page requires you have already subscribed to WoS.
  Shared   
  Discussed   
No Suggested Reading articles found!