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山东大学学报 (工学版) ›› 2022, Vol. 52 ›› Issue (4): 1-11.doi: 10.6040/j.issn.1672-3961.0.2022.009

• 专家约稿 •    下一篇

工程纳米材料颗粒物气溶胶制备方法研究进展

胡卉1(),汤宁业2,*(),王司宇2,王海森2   

  1. 1. 长安大学运输工程学院, 陕西 西安 710064
    2. 长安大学汽车学院, 陕西 西安 710064
  • 收稿日期:2022-04-14 出版日期:2022-08-20 发布日期:2022-08-24
  • 通讯作者: 汤宁业 E-mail:huhui@chd.edu.cn;2020222023@chd.edu.cn
  • 作者简介:胡卉，工学博士，博士后，教授，博士生导师。美国威斯康辛大学麦迪逊分校访问学者。中国物流学会会员，WTC“客运规划与联程运输”技术委员会委员。近5年主持完成国家科技支撑计划项目、陕西省自然科学基础研究计划面上项目、西安市社科重大课题等纵向课题；发表高水平学术论文20余篇，其中SCI 4篇，EI 10余篇。全国大学生物流设计大赛一等奖、陕西省“挑战杯”一等奖指导教师。长安大学国家一流专业骨干，参与制定交通运输部行业标准1项，参编论著3本。
    胡卉(1979—)，女，辽宁锦州人，博士生导师，教授，工学博士，主要研究方向为系统工程。E-mail: huhui@chd.edu.cn
  • 基金资助:
    国家重点研发计划中国和美国政府间合作资助项目(2019YFE0117800)

Research progress on preparation methods of engineering nano material particle aerosol

Hui HU1(),Ningye TANG2,*(),Siyu WANG2,Haisen WANG2   

  1. 1. School of Transportation Engineering, Chang′an University, Xi′an 710064, Shaanxi, China
    2. School of Automobile, Chang′an University, Xi′an 710064, Shaanxi, China
  • Received:2022-04-14 Online:2022-08-20 Published:2022-08-24
  • Contact: Ningye TANG E-mail:huhui@chd.edu.cn;2020222023@chd.edu.cn

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摘要：

随着纳米技术和生物化学领域的发展, 对微观粒子的粒径和制造工艺提出更高的要求。气溶胶作为常见的工程纳米材料颗粒物, 在社会各行各业应用广泛。从气溶胶制备方法出发, 通过对大量相关文献的系统梳理, 综述气溶胶常用制备方法的研究进展, 对比分析不同气溶胶制备方法的适用场景, 明确不同气溶胶制备方法的使用要求, 归纳概述不同气溶胶制备方法的优缺点。在此基础上, 进一步综述不同时期国内外学者对各类方法的优化和完善, 深入剖析国内外学者的试验和研究成果, 对超临界流体技术在气溶胶制备中的应用进行分析与展望。

关键词: 工程纳米材料, 气溶胶, 气溶胶制备, 超临界流体技术, 高压静电雾化

Abstract:

With the development of nanotechnology and biochemistry, higher requirements were put forward for the particle size and manufacturing process of micro particles. Aerosol, as a common engineering nano material particle, was widely used in all walks of life. The research progress of common aerosol preparation methods, which starts from the aerosol preparation methods and systematically based on a large number of relevant literatures, the applicable scenarios of different aerosol preparation methods, the application requirements were summarized of different aerosol preparation methods were defined, the advantages and disadvantages of were compared and analyzed different aerosol preparation methods. On this basis, the optimization and improvement of various methods by domestic and foreign scholars in different periods were further ummarized, and the experimental and research results of domestic and foreign scholars were deeply analyzed, and the application of supercritical fluid technology in aerosol preparation was analyzed and prospected.

Key words: engineering nano materials, aerosol, aerosol preparation, supercritical fluid technology, high voltage electrostatic atomization

中图分类号: 

  • X513

图1

流化床气溶胶发生装置示意图"

图2

气溶胶制备器原理图"

图3

气溶胶制备装置流程图"

图4

高压静电雾化法原理图"

图5

超临界流体辅助雾化法器件示意图"

图6

气溶胶水解法流程图"

图7

加热管和不锈钢毛细管装配结构"

图8

加热气溶胶发生器系统结构"

图9

加热器封装结构"

图10

高压静电雾化装置原理流程图"

图11

静电雾化设备装置图"

图12

不同类型的气溶胶发生器"

表1

不同气溶胶制备方法的特征"

方法 粒径 应用范围 优点 缺点
流化床法 纳米级 固体、液体、气体 应用范围广, 操作简单 粒径大小难以控制且不均匀
雾化法 纳米级 少部分能够溶解于液体的材料 制备工艺高 材料要求高, 应用范围小
凝集法 纳米级 容易发生物理化学反应的固体材料 制备工艺高 材料要求高, 发生器结构复杂, 操作繁琐
高压静电雾化 纳米级 液体和少部分能够溶解于液体的材料 胶粒径小, 分布均匀 质量浓度低, 不能长时间制备
超临界流体雾化 纳米级 液体 粒径分布均匀、制造过程便捷、适用范围广 对试验装置要求较高
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